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By Anil K. Mukherji, R. Belcher and M. Frieser (Auth.)

ISBN-10: 0080068863

ISBN-13: 9780080068862

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A. and KLINGENBURG, J. , Anal. Chem. 27, 835 (1955). VERMA, M. R. and PAUL, S. D . , Nature, 173,1237 (1954). KLINGENBURG, J. , and PAPUCCI, R. , Anal. Chem. 24, 1861 (1952). ALIMARIN, I. P. and HAN-SI, SHEN, Zhur. Anal. Khim. 16, 279 (1961). HAHN, R. B. and JOSEPH, P. , Anal. Chem. 28, 2019 (1956). 101. VENKATARAMANIAH, M. and RAGHAVA RAO, B. S. , / . Indian Chem. Soc. 28, 257 (1951). 102. RYAN, D . , Canadian J. Chem. 38, 2488 (1960). 103. ALIMARIN, I. P. and TUNG-SCHAING, TSE, Talanta, 9, 9 (1962).

Indian Chem. Soc. 28, 257 (1951). 102. RYAN, D . , Canadian J. Chem. 38, 2488 (1960). 103. ALIMARIN, I. P. and TUNG-SCHAING, TSE, Talanta, 9, 9 (1962). 104. 105. 106. 107. 108. 109. 110. 111. 112. BAIULESCU, G. , Anal. Chim. Acta, 21, 33 (1959). ELVING, P. J. and OLSON, E. C , Anal Chem. 27, 1817 (1955). LUNDELL, G. E. F. and KNOWLES, H. , Ind. Engng. Chem. 12, 344 (1920). , Z. Anorg. Chem. 72, 89 (1911). SMITH, G. , Cupferron and Neocupferron, G. F. Smith, Columbus, Ohio, 1938. THORNTON, W.

Place the centrifuge tube in an ice bath and add ammonia (sp. gr. 88) slowly with stirring until the solution is alkaline to litmus (Note 2). Add 5 ml of 100 vol. HfcOa and stir for 5 min. Centrifuge for 5 min at 1500 rpm. Decant the supernatant through a Whatman 40 filter paper. Wash the precipitate with 2 % NH4C1 solution, centrifuge, and decant the supernatant through the filter paper. Pour 20 ml of hot 1:1 v/v HC1 to the centrifuge tube. Swirl to dissolve the precipitate and transfer to a 400 ml beaker.

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Analytical Chemistry of Zirconium and Hafnium by Anil K. Mukherji, R. Belcher and M. Frieser (Auth.)


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